Green synthesis of palladium nanoparticles using fenugreek tea and their catalytic applications in organic reactions

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Abstract

In this communication, we present the fenugreek tea aided green synthesis of Pd nanoparticles (PdNPs@FT). The synthesized PdNPs were characterized by UV–Visible spectroscopy, scanning electron microscopy (SEM), small area electron diffraction (SAED), fourier transform infrared spectroscopy (FT-IR) and X-ray diffraction (XRD). FT-IR manifested that polyol and amide groups present in fenugreek may have participated in the synthesis of palladium nanoparticles. PdNPs@FT exhibited high catalytic activity towards hydrogenation of 4-nitrophenol to 4-aminophenol. PdNPs@FT catalyzed Suzuki–Miyaura coupling reaction between bromobenzene and phenyl boronic acid gave desired biphenyl in excellent yield.

Original languageEnglish
Pages (from-to)138-141
Number of pages4
JournalMaterials Letters
Volume205
DOIs
StatePublished - 15 Oct 2017

Keywords

  • FTIR
  • Green catalyst
  • Nanoparticles
  • Nitrophenol
  • Suzuki-Miyaura reaction

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