Structural, thermal, dielectric and magnetic properties of NiFe 2O 4 nanoleaf

P. Sivakumar; R. Ramesh; A. Ramanand; S. Ponnusamy; C. Muthamizhchelvan

doi:10.1016/j.jallcom.2012.05.067

Structural, thermal, dielectric and magnetic properties of NiFe ₂O ₄ nanoleaf

P. Sivakumar
, R. Ramesh
, A. Ramanand
, S. Ponnusamy
, C. Muthamizhchelvan

Department of Chemistry

Research output: Contribution to journal › Article › peer-review

31 Scopus citations

Abstract

The leaf-like NiFe ₂O ₄ nanostructure formed from nanoparticles has been successfully prepared on polymer assisted sol-gel method. Here ethylene glycol (EG) is used as a gelling agent as well as solvent and PVA as a capping agent. A sequence of control experiments confirms that the polymer concentration with NiFe ₂O ₄ has direct influence on the morphology of the products. Characterization of the synthesized nanoparticles and nanoleaf are carried out using powder XRD, FT-IR, TGA, HR-SEM, TEM, HR-TEM, dielectric measurements tangent, microRaman and VSM. On the basis of these experimental results, potential influence mechanisms in the growth processes are proposed.

Original language	English
Pages (from-to)	203-207
Number of pages	5
Journal	Journal of Alloys and Compounds
Volume	537
DOIs	https://doi.org/10.1016/j.jallcom.2012.05.067
State	Published - 5 Oct 2012

Keywords

Magnetic measurements
Nanostructured materials
Sol-gel processes
Transmission electron microscopy
X-ray diffraction

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10.1016/j.jallcom.2012.05.067

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title = "Structural, thermal, dielectric and magnetic properties of NiFe 2O 4 nanoleaf",

abstract = "The leaf-like NiFe 2O 4 nanostructure formed from nanoparticles has been successfully prepared on polymer assisted sol-gel method. Here ethylene glycol (EG) is used as a gelling agent as well as solvent and PVA as a capping agent. A sequence of control experiments confirms that the polymer concentration with NiFe 2O 4 has direct influence on the morphology of the products. Characterization of the synthesized nanoparticles and nanoleaf are carried out using powder XRD, FT-IR, TGA, HR-SEM, TEM, HR-TEM, dielectric measurements tangent, microRaman and VSM. On the basis of these experimental results, potential influence mechanisms in the growth processes are proposed.",

keywords = "Magnetic measurements, Nanostructured materials, Sol-gel processes, Transmission electron microscopy, X-ray diffraction",

author = "P. Sivakumar and R. Ramesh and A. Ramanand and S. Ponnusamy and C. Muthamizhchelvan",

year = "2012",

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T1 - Structural, thermal, dielectric and magnetic properties of NiFe 2O 4 nanoleaf

AU - Sivakumar, P.

AU - Ramesh, R.

AU - Ramanand, A.

AU - Ponnusamy, S.

AU - Muthamizhchelvan, C.

PY - 2012/10/5

Y1 - 2012/10/5

N2 - The leaf-like NiFe 2O 4 nanostructure formed from nanoparticles has been successfully prepared on polymer assisted sol-gel method. Here ethylene glycol (EG) is used as a gelling agent as well as solvent and PVA as a capping agent. A sequence of control experiments confirms that the polymer concentration with NiFe 2O 4 has direct influence on the morphology of the products. Characterization of the synthesized nanoparticles and nanoleaf are carried out using powder XRD, FT-IR, TGA, HR-SEM, TEM, HR-TEM, dielectric measurements tangent, microRaman and VSM. On the basis of these experimental results, potential influence mechanisms in the growth processes are proposed.

AB - The leaf-like NiFe 2O 4 nanostructure formed from nanoparticles has been successfully prepared on polymer assisted sol-gel method. Here ethylene glycol (EG) is used as a gelling agent as well as solvent and PVA as a capping agent. A sequence of control experiments confirms that the polymer concentration with NiFe 2O 4 has direct influence on the morphology of the products. Characterization of the synthesized nanoparticles and nanoleaf are carried out using powder XRD, FT-IR, TGA, HR-SEM, TEM, HR-TEM, dielectric measurements tangent, microRaman and VSM. On the basis of these experimental results, potential influence mechanisms in the growth processes are proposed.

KW - Magnetic measurements

KW - Nanostructured materials

KW - Sol-gel processes

KW - Transmission electron microscopy

KW - X-ray diffraction

UR - https://www.scopus.com/pages/publications/84862753376

U2 - 10.1016/j.jallcom.2012.05.067

DO - 10.1016/j.jallcom.2012.05.067

M3 - Article

AN - SCOPUS:84862753376

SN - 0925-8388

VL - 537

SP - 203

EP - 207

JO - Journal of Alloys and Compounds

JF - Journal of Alloys and Compounds

ER -

Structural, thermal, dielectric and magnetic properties of NiFe ₂O ₄ nanoleaf

Abstract

Keywords

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