Synthesis of hybrid cellulose nanocomposite bonded with dopamine SiO2/TiO2 and its antimicrobial activity

Sivalingam Ramesh; Gwang Hoon Kim; Jaehwan Kim; Joo Hyung Kim

doi:10.1117/12.2084511

Synthesis of hybrid cellulose nanocomposite bonded with dopamine SiO₂/TiO₂ and its antimicrobial activity

Sivalingam Ramesh, Gwang Hoon Kim, Jaehwan Kim, Joo Hyung Kim

Department of Mechanical, Robotics and Energy Engineering

Inha University

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

Abstract

Organic-inorganic hybrid material based cellulose was synthesized by the sol-gel approach. The explosion of activity in this area in the past decade has made tremendous progress in industry or academic both fundamental understanding of sol-gel process and applications of new functionalized hybrid materials. In this present research work, we focused on cellulose-dopamine functionalized SiO₂/NiO₂ hybrid nanocomposite by sol-gel process. The cellulose-dopamine hybrid nanocomposite was synthesized via λ-aminopropyltriethoxysilane (λ-APTES) coupling agent by in-situ sol-gel process. The chemical structure of cellulose-amine functionalized dopamine bonding to cellulose structure with covalent cross linking hybrids was confirmed by FTIR spectral analysis. The morphological analysis of cellulose-dopamine nanoSiO₂/NiO₂ hybrid nanocomposite materials was characterized by XRD, SEM and TEM. From this different analysis results indicate that the optical transparency, thermal stability, control morphology of cellulose-dopamine-SiO₂/NiO₂ hybrid nanocomposite. Furthermore cellulose-dopamine-SiO₂/NiO₂ hybrid nanocomposite was tested against pathogenic bacteria for antimicrobial activity.

Original language	English
Title of host publication	Nanosensors, Biosensors, and Info-Tech Sensors and Systems 2015
Editors	Vijay K. Varadan
Publisher	SPIE
Edition	January
ISBN (Electronic)	9781628415377
DOIs	https://doi.org/10.1117/12.2084511
State	Published - 2015
Event	Nanosensors, Biosensors, and Info-Tech Sensors and Systems 2015 - San Diego, United States Duration: 9 Mar 2015 → 11 Mar 2015

Publication series

Name	Proceedings of SPIE - The International Society for Optical Engineering
Number	January
Volume	9434
ISSN (Print)	0277-786X
ISSN (Electronic)	1996-756X

Conference

Conference	Nanosensors, Biosensors, and Info-Tech Sensors and Systems 2015
Country/Territory	United States
City	San Diego
Period	9/03/15 → 11/03/15

Keywords

antimicrobial activity
Cellulose
dopamine
optical transparency
thermal stability

Access to Document

10.1117/12.2084511

Cite this

Ramesh, S., Kim, G. H., Kim, J., & Kim, J. H. (2015). Synthesis of hybrid cellulose nanocomposite bonded with dopamine SiO₂/TiO₂ and its antimicrobial activity. In V. K. Varadan (Ed.), Nanosensors, Biosensors, and Info-Tech Sensors and Systems 2015 (January ed.). Article 943410 (Proceedings of SPIE - The International Society for Optical Engineering; Vol. 9434, No. January). SPIE. https://doi.org/10.1117/12.2084511

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title = "Synthesis of hybrid cellulose nanocomposite bonded with dopamine SiO2/TiO2 and its antimicrobial activity",

abstract = "Organic-inorganic hybrid material based cellulose was synthesized by the sol-gel approach. The explosion of activity in this area in the past decade has made tremendous progress in industry or academic both fundamental understanding of sol-gel process and applications of new functionalized hybrid materials. In this present research work, we focused on cellulose-dopamine functionalized SiO2/NiO2 hybrid nanocomposite by sol-gel process. The cellulose-dopamine hybrid nanocomposite was synthesized via λ-aminopropyltriethoxysilane (λ-APTES) coupling agent by in-situ sol-gel process. The chemical structure of cellulose-amine functionalized dopamine bonding to cellulose structure with covalent cross linking hybrids was confirmed by FTIR spectral analysis. The morphological analysis of cellulose-dopamine nanoSiO2/NiO2 hybrid nanocomposite materials was characterized by XRD, SEM and TEM. From this different analysis results indicate that the optical transparency, thermal stability, control morphology of cellulose-dopamine-SiO2/NiO2 hybrid nanocomposite. Furthermore cellulose-dopamine-SiO2/NiO2 hybrid nanocomposite was tested against pathogenic bacteria for antimicrobial activity.",

keywords = "antimicrobial activity, Cellulose, dopamine, optical transparency, thermal stability",

author = "Sivalingam Ramesh and Kim, {Gwang Hoon} and Jaehwan Kim and Kim, {Joo Hyung}",

note = "Publisher Copyright: {\textcopyright} 2015 SPIE.; Nanosensors, Biosensors, and Info-Tech Sensors and Systems 2015 ; Conference date: 09-03-2015 Through 11-03-2015",

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Ramesh, S, Kim, GH, Kim, J & Kim, JH 2015, Synthesis of hybrid cellulose nanocomposite bonded with dopamine SiO₂/TiO₂ and its antimicrobial activity. in VK Varadan (ed.), Nanosensors, Biosensors, and Info-Tech Sensors and Systems 2015. January edn, 943410, Proceedings of SPIE - The International Society for Optical Engineering, no. January, vol. 9434, SPIE, Nanosensors, Biosensors, and Info-Tech Sensors and Systems 2015, San Diego, United States, 9/03/15. https://doi.org/10.1117/12.2084511

Synthesis of hybrid cellulose nanocomposite bonded with dopamine SiO₂/TiO₂ and its antimicrobial activity. / Ramesh, Sivalingam; Kim, Gwang Hoon; Kim, Jaehwan et al.
Nanosensors, Biosensors, and Info-Tech Sensors and Systems 2015. ed. / Vijay K. Varadan. January. ed. SPIE, 2015. 943410 (Proceedings of SPIE - The International Society for Optical Engineering; Vol. 9434, No. January).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

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AB - Organic-inorganic hybrid material based cellulose was synthesized by the sol-gel approach. The explosion of activity in this area in the past decade has made tremendous progress in industry or academic both fundamental understanding of sol-gel process and applications of new functionalized hybrid materials. In this present research work, we focused on cellulose-dopamine functionalized SiO2/NiO2 hybrid nanocomposite by sol-gel process. The cellulose-dopamine hybrid nanocomposite was synthesized via λ-aminopropyltriethoxysilane (λ-APTES) coupling agent by in-situ sol-gel process. The chemical structure of cellulose-amine functionalized dopamine bonding to cellulose structure with covalent cross linking hybrids was confirmed by FTIR spectral analysis. The morphological analysis of cellulose-dopamine nanoSiO2/NiO2 hybrid nanocomposite materials was characterized by XRD, SEM and TEM. From this different analysis results indicate that the optical transparency, thermal stability, control morphology of cellulose-dopamine-SiO2/NiO2 hybrid nanocomposite. Furthermore cellulose-dopamine-SiO2/NiO2 hybrid nanocomposite was tested against pathogenic bacteria for antimicrobial activity.

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