Synthesis of multi-linked ZnO rods by microwave heating

A. Kathalingam; Y. S. Chae; J. K. Rhee

doi:10.1002/crat.201100097

Synthesis of multi-linked ZnO rods by microwave heating

A. Kathalingam, Y. S. Chae, J. K. Rhee

Millimeterwave Innovation Technology Research Center

Dongguk University

Research output: Contribution to journal › Article › peer-review

20 Scopus citations

Abstract

Synthesis of linked ZnO micro rods by microwave radiation and its characterization is presented in this report. In this simple microwave assisted solution phase route zinc nitrate and hexamethylenetetramine has been used as the starting materials for the synthesis of linked ZnO rods. Linked ZnO rods with various morphologies such as bipods, tripods, tetrapods and etc have been prepared. The influence of irradiation time of microwave on the formation of linked ZnO rods was investigated. X-ray powder diffraction (XRD), field emission scanning electron microscopy (FESEM), and energy dispersive spectroscopy (EDS) were used for the characterization of the product. The FESEM images showed ZnO rods of diameter in the range of 100-200 nm and length around 5000 nm.

Original language	English
Pages (from-to)	517-522
Number of pages	6
Journal	Crystal Research and Technology
Volume	46
Issue number	5
DOIs	https://doi.org/10.1002/crat.201100097
State	Published - May 2011

Keywords

linked rods
microwave synthesis
optical properties and photoluminescence
zinc oxide

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10.1002/crat.201100097

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abstract = "Synthesis of linked ZnO micro rods by microwave radiation and its characterization is presented in this report. In this simple microwave assisted solution phase route zinc nitrate and hexamethylenetetramine has been used as the starting materials for the synthesis of linked ZnO rods. Linked ZnO rods with various morphologies such as bipods, tripods, tetrapods and etc have been prepared. The influence of irradiation time of microwave on the formation of linked ZnO rods was investigated. X-ray powder diffraction (XRD), field emission scanning electron microscopy (FESEM), and energy dispersive spectroscopy (EDS) were used for the characterization of the product. The FESEM images showed ZnO rods of diameter in the range of 100-200 nm and length around 5000 nm.",

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N2 - Synthesis of linked ZnO micro rods by microwave radiation and its characterization is presented in this report. In this simple microwave assisted solution phase route zinc nitrate and hexamethylenetetramine has been used as the starting materials for the synthesis of linked ZnO rods. Linked ZnO rods with various morphologies such as bipods, tripods, tetrapods and etc have been prepared. The influence of irradiation time of microwave on the formation of linked ZnO rods was investigated. X-ray powder diffraction (XRD), field emission scanning electron microscopy (FESEM), and energy dispersive spectroscopy (EDS) were used for the characterization of the product. The FESEM images showed ZnO rods of diameter in the range of 100-200 nm and length around 5000 nm.

AB - Synthesis of linked ZnO micro rods by microwave radiation and its characterization is presented in this report. In this simple microwave assisted solution phase route zinc nitrate and hexamethylenetetramine has been used as the starting materials for the synthesis of linked ZnO rods. Linked ZnO rods with various morphologies such as bipods, tripods, tetrapods and etc have been prepared. The influence of irradiation time of microwave on the formation of linked ZnO rods was investigated. X-ray powder diffraction (XRD), field emission scanning electron microscopy (FESEM), and energy dispersive spectroscopy (EDS) were used for the characterization of the product. The FESEM images showed ZnO rods of diameter in the range of 100-200 nm and length around 5000 nm.

KW - linked rods

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KW - optical properties and photoluminescence

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Synthesis of multi-linked ZnO rods by microwave heating

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Keywords

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