TY - JOUR
T1 - Synthesis of novel Sn1-xZnxO-chitosan nanocomposites
T2 - Structural, morphological and luminescence properties and investigation of antibacterial properties
AU - Packirisamy, Rajiv Gandhi
AU - Govindasamy, Chandramohan
AU - Sanmugam, Anandhavelu
AU - Venkatesan, Sethuraman
AU - Kim, Hyun Seok
AU - Vikraman, Dhanasekaran
N1 - Publisher Copyright:
© 2019 Elsevier B.V.
PY - 2019/10/1
Y1 - 2019/10/1
N2 - In recent times, metal oxide-organic nanocomposites have received great attention because of their feasibility to wide range applications such as super capacitors, antibacterial activity, biomedical sensors, battery applications and microfluidic devices. In this work, zinc oxide-chitosan (ZnO-CS) and their novel tin zinc oxide-chitosan (Sn1-xZnxO-CS) hybrid nanocomposites successfully synthesized by a simple one-pot sol-gel reaction. The equal metal oxide ratio such as 0.5, 1.0, 1.5 and 2.0% (W/V) for zinc and tin sources with constant weight of chitosan were used to prepare the Sn1-xZnxO-CS nanocomposites. Fourier transform infrared spectroscopy results proved the formation of Sn1-xZnxO-CS nanocomposites. X-ray diffraction patterns discovered the mixed phase polycrystalline nature of Sn1-xZnxO-CS nanocomposites. Optical and luminescence properties were extensively studied for nanocomposites by UV–Vis and photoluminescence spectroscopy, respectively. The surface modification elaborately discussed with scanning electron microscope images due to incorporation of SnOx with ZnO-CS matrix. The antibacterial properties of Sn1-xZnxO-CS were tested against Escherichia coli, Salmonella Typhi and Klebseilla Pneumoniae bacterial species.
AB - In recent times, metal oxide-organic nanocomposites have received great attention because of their feasibility to wide range applications such as super capacitors, antibacterial activity, biomedical sensors, battery applications and microfluidic devices. In this work, zinc oxide-chitosan (ZnO-CS) and their novel tin zinc oxide-chitosan (Sn1-xZnxO-CS) hybrid nanocomposites successfully synthesized by a simple one-pot sol-gel reaction. The equal metal oxide ratio such as 0.5, 1.0, 1.5 and 2.0% (W/V) for zinc and tin sources with constant weight of chitosan were used to prepare the Sn1-xZnxO-CS nanocomposites. Fourier transform infrared spectroscopy results proved the formation of Sn1-xZnxO-CS nanocomposites. X-ray diffraction patterns discovered the mixed phase polycrystalline nature of Sn1-xZnxO-CS nanocomposites. Optical and luminescence properties were extensively studied for nanocomposites by UV–Vis and photoluminescence spectroscopy, respectively. The surface modification elaborately discussed with scanning electron microscope images due to incorporation of SnOx with ZnO-CS matrix. The antibacterial properties of Sn1-xZnxO-CS were tested against Escherichia coli, Salmonella Typhi and Klebseilla Pneumoniae bacterial species.
KW - Antibacterial
KW - Chitosan
KW - Nanocomposites
KW - SnZnO
KW - ZnO
UR - http://www.scopus.com/inward/record.url?scp=85069629461&partnerID=8YFLogxK
U2 - 10.1016/j.ijbiomac.2019.07.120
DO - 10.1016/j.ijbiomac.2019.07.120
M3 - Article
C2 - 31336118
AN - SCOPUS:85069629461
SN - 0141-8130
VL - 138
SP - 546
EP - 555
JO - International Journal of Biological Macromolecules
JF - International Journal of Biological Macromolecules
ER -